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NITRIC ACID
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Nitric acid is used in the preparation of many explosives, incendiary mixtures, and acid
delay timers. It may be prepared by distilling a mixture of potassium nitrate and concentrated
sulfuric acid.
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MATERIALS
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Potassium nitrate (2 parts by volume).
Two bottles or ceramic jugs (narrow necks
are preferable.)
Pot or frying pan.
Heat source (wood, coal, or charcoal.)
Tape
(paper, electrical, masking, etc., but not cellophane.)
Paper or rags.
Sources:
Drug Store. Motor vehicle batteries, Industrial plants.
IMPORTANT: If sulfuric acid is
obtained from a motor vehicle battery, concentrate it by boiling it until white fumes appear. DO NOT
INHALE FUMES.
NOTE: The amount of nitric acid produced is the same as the amount of potassium
nitrate. Thus, for 2 tablespoonsful of nitric acid, use 2 tablespoonsful of potassium nitrate and 1
tablespoonful of concentrated sulfuric acid.
PROCEDURE:
1. Place dry potassium
nitrate in bottle or jug. Add sulfuric acid. Do not fill bottle more than 1/4 full. Mix until paste
is formed.
CAUTION: Sulfuric acid will burn skin and destroy clothing. If any is
spilled, wash it away with a large quantity of water. Fumes are also dangerous and should not be
inhaled.
2. Wrap paper or rages around necks of the 2 bottles. Securely tape necks of
bottles together. Be sure bottles are flush against each other and that there are no air spaces.
Paper and tape -\
|————\ | /————|
| \___=======___/ |
|
bottle A ___|||||||___ bottle B |
|=============/ ======= \ |
———-|–/
\————|
|||||||| \– Sulfuric acid ||||||||
||| ||| & Potassium Nitrate |||
|||
\—— Supports ———-/
Bottle B should be slightly lower than bottle A,
but not so low as to let the
paste to flow from A to B.
3. Support bottles on
rocks or cans so that empty bottle is SLIGHTLY lower that bottle containing past so that nitric acid
that is formed in receiving bottle will not run into other bottle.
4. Build fire in pot
or frying pan.
5. Gently heat bottle containing mixture by moving fire in and out. As
red fume begin to appear periodically pour cool water over empty receiving bottle. Nitric acid will
begin to form in the receiving bottle.
CAUTION: Do not overheat or wet bottle
containing mixture or it may shatter. As an added precaution, place bottle to be heated in a heat
resistant container filled with sand or gravel. Heat this outer container to produce nitric acid.
/———-\ /- Tape Seal
| |-\ | /————|
| | \___=======___/ |
|
Can | ___|||||||___ bottle B |
^| |==/ | ======= \ |
^^| |-/ \-Bottle A
\————|
^^^\———-/ ||||||||
FIRE ||||||| \– Heat resistant |||rock|
\—-/|| ||| container filled with ||| |||
sand or gravel
6. Continue the above
process until no more red fumes are formed. If the nitric acid formed in the receiving bottle is not
clear (cloudy) pour it into cleaned bottle and repeat Steps 2-6.
CAUTION: Nitric
acid will burn skin and destroy clothing. If any is spilled, wash it away with a large quantity of
water. Fumes are also dangerous and should not be inhaled.
Nitric acid should be kept
away from all combustibles and should be kept in a SEALED CERAMIC OR GLASS container. 03-31
Cellulose Nitrate is known as smokeless powder. It doesn’t take much time or
effort to make it
and can be useful for use indoors where you don’t want any
smoke left floating around the
room.
Materials
———
Concentrated Sulfuric Acid
Concentrated
Nitric Acid
Absorbent Cotton
Sodium Bicarbonate
A 250ml Beaker
Ice Bath
Tongs
Procedure
———
Put the beaker in the ice
bath. Add 70ml of Sulfuric Acid, and 30ml of
Nitric Acid.
Divide the cotton into 7/10
gram pieces. Use the tongs to submerge each
piece of the cotton into the acid solution for 1
minute.
Rinse each piece of cotton in 3 successive baths of water, each bath
containing
500ml of water. Use fresh water for each piece.
Now, immerse the cotton into 250ml of Sodium
Bicarbonate. If it bubbles
rinse it in fresh water once more and contiue the procedure until
no bubbling
occurs.
Squeeze each piece dry and put it on paper towels overnight.
You already know what you are supposed to do with it now. Have fun…
[bad boy
in black]
Have fun with this.. iI included the nitric ascid recipe because it is so
hare d to get normally.. Alpine Kracker
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