Acetone Peroxide I've posted this exact tutorial many places, here we go...
Acetone Peroxide = C9H18O6
Acetone Peroxide is a Primary High Explosive. It is sensitive to shock, heat, light, friction, and most other things an explosive can be sensitive to. This isn't much of a problem if you handle it with care and when you're making it you add the HCl in slowly, drop wise. If this is done, Acetone Peroxide is a great place to start in HE's.
Materials:
Chemicals- 500mL of 3% H2O2 (1), 300mL of 100% Acetone (2), and 250mL of 20-30% HCl (3).
Equipment- large glass container (jar 1L+), a beaker (500mL+), and some Coffee filters/filter paper.
Procedure:
First take your beaker and fill it with 500 mL of H2O2, dump this into your jar.
Next measure 300 mL of Acetone into the beaker, pour this into the jar.
Now measure the 250 mL of HCl and pour this into the jar drop-wise, very slowly, if the HCl is added too quickly you will end up with dicyclo AP which is very sensitive.
Once this is done place your jar into a refrigerator and leave it there for at least 1 week.
After about a week the jar will have tiny crystals floating on the bottom. These crystals are the AP.
Now it is time to filter, get another jar and cover the opening of it with the filter paper. now pour the liquid into the filter, keep adding until all the liquid is gone and you cant see the crystals in the other jar any more.
After you filter you will need to let the AP dry for awhile, set it in a cool, dark, dry place, do not put it in the oven unless you dont want the oven anymore!
Once it is dry you are ready to pack it into your casing, pack it in tightly but be sure not to pound it in, this could cause it to go off right in your hand. This recipe makes about 15 grams. (I reccomend starting with 5g or under!)
(1) H2O2 can be purchased at any store, H2O2 is also known as hydrogen peroxide, the stuff in the brown bottle that you put on cuts to disinfect them.
(2) Acetone can be purchased at lowes or another hardware store as a paint remover, or as nail varnish remover but the
acetone in nail varnish remover is diluted.
(3) HCl (hydrocloric acid) for this you can use a drain opener, like draino, I recommend "the works" it seems to be the only one with any HCl in it that i can find at my local store.
AP is a very sensitive primary explosive, use with caution.
You can also use H2SO4 for this synthesis instead of HCl, if you use H2SO4 use an ice bath becasue it tends to heat up. |