Does the box you're using say "Ephedrine" or "Pseudo-ephedrine".
Did you crush the pills of just break them?
How long did you let it sit?
Was the water between 25 and 40 degrees C?
It's not magic mike, you don't toss it all in a pot and "bang" - it works instantly.
Try actually looking for the extraction process on other sites - or just google "Guaifenesin soluability".
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